Studies on the SYNTHETIC Method of 2,5-Dihydroxyterephthalaldehyde

Authors

  • Xiang Ji
  • Chunmei Yuan
  • Shengqun Ma

DOI:

https://doi.org/10.54097/pgb2qm78

Abstract

 2,5-Dihydroxyterephthalendehyde (Dha) can be used as an intermediate in organic chemistry and synthetic materials, which can participate in a variety of chemical reactions. Through these reactions, a variety of valuable compounds can be synthesized. However, the existing synthesis methods are cumbersome, difficult to operate, and have low yields. Referring to the reported Dha synthesis process, we successfully synthesized Dha using inexpensive 1,4-dimethoxybenzene with simple steps. The correct structure was proved by Fourier transform infrared (FT-IR) spectroscopy, nuclear magnetic resonance (1H-NMR) hydrogen spectroscopy, and nuclear magnetic resonance (13C CP-MAS NMR) carbon spectroscopy, which provides a valuable reference for the synthesis of Dha.

Downloads

Download data is not yet available.

References

Ke, H., Zhang, Q., Zhang, X., Cheng, G., Sun, Y., Li, J., Cheng, H., 2021. Hydroquinone-based conjugated schiff base polymer as anode material for lithium ion batteries. Materials Letters 286, https://doi.org/10.1016/j.matlet.2020.129235.

Zuo, H., Li, Y., Liao, Y., 2019. Europium ionic liquid grafted covalent organic framework with dual luminescence emissions as sensitive and selective acetone sensor. ACS Applied Materials & Interfaces 11, 39201-39208. https://doi.org/10.1021/acsami.9b14795.

Xia, M., Shen, T., Li, C., Fan, R., Feng, L., Chen, Q., 2022. 2d cofs paper composites fabricated by the in situ growth for visual detection of target metal ions. Materials Chemistry and Physics 286, https://doi.org/10.1016/j.matchemphys.2022.126208.

Li, Y., Zuo, K., Gao, T., Wu, J., Su, X., Zeng, C., Xu, H., Hu, H., Zhang, X., Gao, Y., 2022. Bimetallic docked covalent organic frameworks with high catalytic performance towards coupling/oxidation cascade reactions. RSC Advances 12, 4874-4882. https://doi.org/10.1039/d1ra05315a.

Ma, B., Xu, Y., Hu, F., Zhang, G., Zheng, X., Wang, Z., Qiao, H., Yang, D., Mi, L., 2022. Phenolic hydroxyl‐functionalized covalent–organic frameworks for formal [3+2] reaction. Macromolecular Chemistry and Physics 223, https://doi.org/10.1002/macp.202100462.

Meng, F.-L., Qian, H.-L., Yan, X.-P., 2021. Conjugation-regulating synthesis of high photosensitizing activity porphyrin-based covalent organic frameworks for photodynamic inactivation of bacteria. Talanta 233, https://doi.org/10.1016/j.talanta.2021.122536.

He, Y., Lin, X., 2021. Fabricating compact covalent organic framework membranes with superior performance in dye separation. Journal of Membrane Science 637, https://doi.org/10.1016/j.memsci.2021.119667.

Cheung, P. L., Lee, S. K., Kubiak, C. P., 2019. Facile solvent-free synthesis of thin iron porphyrin cofs on carbon cloth electrodes for co2 reduction. Chemistry of Materials 31, 1908-1919. https://doi.org/10.1021/acs.chemmater.8b04370.

Liu, C., Xu, G., Li, B., Wang, X., Lin, J.-M., Zhao, R.-S., 2023. Three-dimensional hydroxylated covalent organic frameworks for solid phase extraction of glucocorticoids in environmental water samples. Analytica Chimica Acta 1239, https://doi.org/10.1016/j.aca.2022.340662.

Li, W., Shen, M., Yu, Y.-J., Chen, Y.-X., Chen, L., Ren, S.-B., Han, D.-M., 2022. Superhydrophobic covalent organic frameworks prepared via nucleophilic substitution reaction for effective oil/water separation. Colloids and Surfaces A: Physicochemical and Engineering Aspects 655, https://doi.org/10.1016/j.colsurfa.2022.130239.

Downloads

Published

27-04-2024

Issue

Section

Articles

How to Cite

Ji, X., Yuan, C., & Ma, S. (2024). Studies on the SYNTHETIC Method of 2,5-Dihydroxyterephthalaldehyde. Academic Journal of Science and Technology, 10(3), 59-61. https://doi.org/10.54097/pgb2qm78